Laboratory Manual for Organic Chemistry
Edition: 2
Copyright: 2023
Pages: 124
Edition: 2
Copyright: 2023
Pages: 98
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Laboratory Manual for Organic Chemistry, 2nd edition, has been extensively revised from its first edition. All of the exercises, for example, have been modified to improve product yield, better fit within the increasingly common three-hour lab period, and/or minimize hazardous waste generation. In addition to these improvements, four new exercises have been added: a synthesis of biphenyl via a Suzuki-Miyaura coupling reaction, a corresponding exercise that explores substituent effects on the reaction's yield, a chemistry drawing software exercise, and a vanillyl alcohol synthesis. Notably, all of the artwork and reactions from the first edition have been redrawn for ease and clarity. Lastly, the appendix and instructor's manual have been updated.
Lab Safety
Lab Notebooks
Significant Figures & More
Lab Calculations
EXERCISE 1: Chemical Drawing Software
EXERCISE 2: Melting Points
EXERCISE 3: Distillation
EXERCISE 4: Recrystallization
EXERCISE 5: Extraction
EXERCISE 6: Essential Oil Isolation
EXERCISE 7: Paprika Pigment Isolation
EXERCISE 8: d-Limonene Isolation
EXERCISE 9: Methyl Stearate Synthesis
EXERCISE 10: Isoborneol Synthesis
EXERCISE 11: t-Pentyl Chloride Synthesis
EXERCISE 12: Benzopinacolone Synthesis
EXERCISE 13: Wintergreen Synthesis
EXERCISE 14: 1,4-Di-t-butyl-2,5-dimethoxybenzene Synthesis
EXERCISE 15: Biphenyl Synthesis
EXERCISE 16: Biphenyl Synthesis Substituent Affects
EXERCISE 17: Benzocaine Synthesis
EXERCISE 18: Ethanol Synthesis
EXERCISE 19: Nerolin Synthesis
EXERCISE 20: Artificial Flavor Synthesis
EXERCISE 21: Vanillyl Alcohol Synthesis
EXERCISE 22: Sulfa Drug Synthesis
EXERCISE 23: Dibenzalacetone Synthesis
EXERCISE 24: GCMS Analysis of Gasoline
EXERCISE 25: GCMS Analysis of Antihistamines
EXERCISE 26: HPLC Analysis of Analgesics
EXERCISE 27: Alcohol Oxidation Kinetics
APPENDIX