Organic Chemistry I Laboratory Experiments for Chemistry 221

Edition: 2

Copyright: 2025

Pages: 88

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$40.00 USD

ISBN 9798385168330

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The application of experimental techniques for solving chemical problems is essential for a full appreciation of chemistry and for science in general. Success in the lab requires careful preparation—you must read the experiment and complete each pre-lab assignment prior to coming to the lab. Your grade will be based on your performance in the lab, written reports, and your understanding of the chemical principles involved in the experiments. 

The objectives of the laboratory sessions will provide the learners experience to:

  • work safely and comfortably in the lab
  • gain the experience of executing basic laboratory techniques and the use of modern instrumental methods.
  • make careful qualitative observations and obtain reproduceable quantitative data
  • maintain and keep a complete accurate and well-organized record of experimental laboratory work.
  • be able to evaluate experimental and instrumental data.
  • compile a complete laboratory report that includes valid conclusions based on the evaluation of recorded data.

INTRODUCTION
LABORATORY CHECK-IN PROCEDURES

EXPERIMENT 1 Determination of Melting Points
EXPERIMENT 2 Purification of Solids Using Miniscale and Microscale Crystallization Techniques
EXPERIMENT 3 Chromatography
EXPERIMENT 4 Distillation
EXPERIMENT 5 Extraction
EXPERIMENT 6 Infrared Spectroscopy
EXPERIMENT 7 Extraction of Caffeine From Tea Gas Chromatography Analysis
EXPERIMENT 8 The Isomerization of Maleic Acid to Fumaric Acid
EXPERIMENT 9 Synthesis of n-butyl bromide an example of Nucleophilic Substitiution Reaction: SN2
EXPERIMENT 10 Microscale Preparation of Cyclohexene
EXPERIMENT 11 Th e Stereochemistry of the Addition of Bromine to a Double Bond

APPENDIX D

Rayvon Sneed
Catherine Malele
Edward Miskiel

The application of experimental techniques for solving chemical problems is essential for a full appreciation of chemistry and for science in general. Success in the lab requires careful preparation—you must read the experiment and complete each pre-lab assignment prior to coming to the lab. Your grade will be based on your performance in the lab, written reports, and your understanding of the chemical principles involved in the experiments. 

The objectives of the laboratory sessions will provide the learners experience to:

  • work safely and comfortably in the lab
  • gain the experience of executing basic laboratory techniques and the use of modern instrumental methods.
  • make careful qualitative observations and obtain reproduceable quantitative data
  • maintain and keep a complete accurate and well-organized record of experimental laboratory work.
  • be able to evaluate experimental and instrumental data.
  • compile a complete laboratory report that includes valid conclusions based on the evaluation of recorded data.

INTRODUCTION
LABORATORY CHECK-IN PROCEDURES

EXPERIMENT 1 Determination of Melting Points
EXPERIMENT 2 Purification of Solids Using Miniscale and Microscale Crystallization Techniques
EXPERIMENT 3 Chromatography
EXPERIMENT 4 Distillation
EXPERIMENT 5 Extraction
EXPERIMENT 6 Infrared Spectroscopy
EXPERIMENT 7 Extraction of Caffeine From Tea Gas Chromatography Analysis
EXPERIMENT 8 The Isomerization of Maleic Acid to Fumaric Acid
EXPERIMENT 9 Synthesis of n-butyl bromide an example of Nucleophilic Substitiution Reaction: SN2
EXPERIMENT 10 Microscale Preparation of Cyclohexene
EXPERIMENT 11 Th e Stereochemistry of the Addition of Bromine to a Double Bond

APPENDIX D

Rayvon Sneed
Catherine Malele
Edward Miskiel